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Durable press finishing of cotton with polycarboxylic acids. I. Preparation of thiosuccinyl‐ s ‐triazine
Author(s) -
Lewis D. M.,
Voncina B.
Publication year - 1997
Publication title -
journal of applied polymer science
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.575
H-Index - 166
eISSN - 1097-4628
pISSN - 0021-8995
DOI - 10.1002/(sici)1097-4628(19971121)66:8<1465::aid-app7>3.0.co;2-c
Subject(s) - cyanuric chloride , capillary electrophoresis , cyanuric acid , reagent , polymer chemistry , fourier transform infrared spectroscopy , chemistry , triazine , derivative (finance) , infrared spectroscopy , chloride , organic chemistry , nuclear chemistry , melamine , chromatography , chemical engineering , engineering , economics , financial economics
The preparation of an alternative polycarboxylic acid to replace the most promising, but expensive, crosslinking reagent 1,2,3,4‐butanetetracarboxylic acid (BTCA) is reported. The reaction of mercaptosuccinic acid with 2,4,6‐trichloro‐ s ‐triazine (cyanuric chloride) gave a dithiosuccinyl derivative. The preparation reaction was followed using horizontal ATR infrared spectroscopy and capillary electrophoresis. The final product was characterized by FTIR, capillary electrophoresis, and 1 H‐NMR. © 1997 John Wiley & Sons, Inc. J Appl Polym Sci 66: 1465–1474, 1997