Premium
1 H and 13 C NMR spectral assignments of some tetracyclic phenothiazine derivatives
Author(s) -
Chatel F.,
Faure R.,
Boyer G.,
Galy J. P.
Publication year - 2000
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/(sici)1097-458x(200002)38:2<137::aid-mrc596>3.0.co;2-7
Subject(s) - heteronuclear molecule , chemistry , phenothiazine , diphenylamine , carbon 13 nmr , chemical shift , stereochemistry , heteronuclear single quantum coherence spectroscopy , proton nmr , two dimensional nuclear magnetic resonance spectroscopy , nuclear magnetic resonance spectroscopy , organic chemistry , medicine , pharmacology
The 1 H and 13 C NMR resonances of 12 tetracyclic phenothiazine derivatives were completely and unequivocally assigned by the concerted application of 1 H‐detected heteronuclear one‐bond (gs‐HMQC) and long‐range (gs‐HMBC) gradient selected correlation experiments. 1 H and 13 C chemical shifts are also reported for the respective diphenylamine precursors. Copyright © 2000 John Wiley & Sons, Ltd.