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Complete assignment of 1 H and 13 C NMR spectra of a set of sulphinyl and sulphonyl monomers toward poly( p ‐phenylenevinylene) precursors
Author(s) -
Breemen Albert J. J. M. van,
Adriaensens Peter J.,
Issaris Anna C. J.,
Kok Margreet M. de,
Vanderzande Dirk J. M.,
Gelan Jan M. J. V.
Publication year - 2000
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/(sici)1097-458x(200002)38:2<129::aid-mrc602>3.0.co;2-k
Subject(s) - chemistry , monomer , carbon 13 nmr , proton nmr , spectral line , nuclear magnetic resonance spectroscopy , nmr spectra database , stereochemistry , polymer chemistry , organic chemistry , polymer , physics , astronomy
The complete assignment of the 1 H and 13 C NMR spectra of sulphinyl and sulphonyl monomers toward poly( p ‐phenylenevinylene) precursors is presented. For all compounds the same protocol could be used. Resonance assignments were achieved by the use of one‐ and two dimensional NMR techniques such as 1 H, 13 C APT and 2D HETCOR ( J = 8 Hz, J = 140 Hz), INADEQUATE and COSY. Copyright © 2000 John Wiley & Sons, Ltd.