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1 H and 13 C NMR Spectroscopy analysis of acetonides of D ‐Glucitol Derivatives
Author(s) -
Kato Lucilia,
Braga Raquel Marques
Publication year - 1999
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/(sici)1097-458x(199906)37:6<447::aid-mrc476>3.0.co;2-l
Subject(s) - chemistry , nuclear magnetic resonance spectroscopy , carbon 13 nmr satellite , nmr spectra database , carbon 13 nmr , proton nmr , spectral line , fluorine 19 nmr , spectroscopy , stereochemistry , physics , quantum mechanics , astronomy
A series of acetonides was obtained during the formal synthesis of deoxynojirimycin. The 1 H NMR spectra of these derivatives contain strongly coupled multiplets covering a chemical shift range of about 1 ppm. The spectra are severely complicated by second‐order effects and were assigned by 2D NMR and 13 C NMR experiments. Copyright © 1999 John Wiley & Sons, Ltd.