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Analysis of 1 H and 13 C NMR Spectra of cis ‐ and trans ‐10‐Chlorodecal‐2‐ones by 2D NMR Techniques
Author(s) -
Di Maio G.,
Iavarone C.,
Migneco L. M.,
Vecchi E.
Publication year - 1996
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/(sici)1097-458x(199601)34:1<18::aid-omr838>3.0.co;2-r
Subject(s) - chemistry , spectral line , nmr spectra database , carbon 13 nmr , carbon 13 nmr satellite , two dimensional nuclear magnetic resonance spectroscopy , decoupling (probability) , proton nmr , nuclear magnetic resonance spectroscopy , stereochemistry , nuclear magnetic resonance , computational chemistry , analytical chemistry (journal) , fluorine 19 nmr , organic chemistry , physics , astronomy , control engineering , engineering
The 1 H and 13 C NMR chemical shift assignments of trans ‐ and cis ‐10‐chlorodecal‐2‐ones were based on 2D COSY and HETCOR experiments. The spectra were measured either in CDCl 3 or in C 6 D 6 to optimize the spectral dispersion (ASIS effect). Selective spin decoupling experiments were also performed.