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− The electrochemical behavior of Nd 2 O 3 -La 2 O 3 -NiO mixed oxide including rare earth resources has been studied to synthesize La 0.5 Nd 0.5 Ni 5 alloy in a LiCl molten salt. The Nd 2 O 3 -La 2 O 3 -NiO mixed oxide was converted to NiNd 2 O 4 (spinel) and LaNiO 3 (perovskite) structures at a sintering temperature of 1100 C. The spinel and perovskite structures led a speed-up in the electrolytic reduction of the mixed oxide. Various reaction intermediates such as Ni, NiLa 2 O 4 were observed during the electrochemical reduction by XRD analysis. A possible reaction route to La 0.5 Nd 0.5 Ni 5 in the LiCl molten salt was proposed based on the analysis result.

Preparation of La0.5Nd0.5Ni5Alloy by an Electrochemical Reduction in Molten LiCl

Preparation of La_0.5Nd_0.5Ni₅Alloy by an Electrochemical Reduction in Molten LiCl