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Recycling of Cutting Oil from Silicon Waste Sludge of Solar Wafer
Author(s) -
Myeong-Heon Um,
Jong-Jib Lee,
Beom Yong Ha
Publication year - 2016
Publication title -
clean technology
Language(s) - English
Resource type - Journals
eISSN - 2288-0690
pISSN - 1598-9712
DOI - 10.7464/ksct.2016.22.4.274
Subject(s) - reagent , materials science , turbidity , wafer , silicon , metal , acetone , chemistry , nuclear chemistry , waste management , metallurgy , organic chemistry , oceanography , geology , engineering , nanotechnology
In this study, it was to develop a chemical method that can recycle the cutting oil which accounts for about 25% of the cost of the process among containing materials of silicon waste sludge generated in the process for producing a solar cell wafer. The 7 types of reagents have been used, including acetone, HCl, NaOH, KOH, Na2CO3, HF, CH2Cl2, etc. for this experiment. And It was carried out at a speed of 3000 rpm for 60 minutes centrifugation after performing a reaction with a waste sludge at various concentrations. As a result, the best reagents and conditions for separating the solid such as a silicon powder and a metal powder and liquid cutting oil were identified as 0.3 N NaOH. It is found to be pH 6.05 in a post-processing recycled cutting oil with 0.3 N NaOH after reaction of waste sludge and 0.1 N HCl which is effective to remove metal powder in order to adjust the pH to suit the properties of the weak acid is a commercially available cutting oil and it showed excellent turbidity than when applied to sludge with 0.3 N NaOH alone. The results of FT-IR analysis which can compare the properties of the commercially available cutting oil shows it has a possibility of recycling oil. The cutting oil recovery rate obtained through the experiment was found to be 86.9%.

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