Visible-Light Promoted Preparation of Trifluoromethylated Tetrahydrofuran and Tetrahydropyran | Zendy

Na Wang | Zendy; QiangShuai Gu | Zendy; YongFeng Cheng | Zendy; Lei Li | Zendy; ZhongLiang Li | Zendy; Zhen Guo | Zendy; XinYuan Liu | Zendy

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Visible-Light Promoted Preparation of Trifluoromethylated Tetrahydrofuran and Tetrahydropyran

Author(s) -

Na Wang,

QiangShuai Gu,

YongFeng Cheng,

Lei Li,

ZhongLiang Li,

Zhen Guo,

XinYuan Liu

Publication year - 2019

Publication title -

chinese journal of organic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.314

H-Index - 33

ISSN - 0253-2786

DOI - 10.6023/cjoc201808048

Subject(s) - chemistry , tetrahydropyran , tetrahydrofuran , organic chemistry , combinatorial chemistry , ring (chemistry) , solvent

An efficient protocol for facile access to trifluoromethylated tetrahydrofuran and tetrahydropyran has been developed under visible light irradiation conditions via radical 1,2-alkoxyl-trifluoromethylation of unactivated alkene. It features the use of readily commercially available and operatively simple trifluoromethanesulfonyl chloride as a trifluoromethyl radical source, thus making the protocol potentially appealing for practical preparation.

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