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Mechanical properties of microwave sintered 8 mol% yttria stabilized zirconia
Author(s) -
Ganesh babu P,
P. Manohar
Publication year - 2013
Publication title -
international journal of the physical sciences
Language(s) - English
Resource type - Journals
ISSN - 1992-1950
DOI - 10.5897/ijps12.549
Subject(s) - materials science , yttria stabilized zirconia , scanning electron microscope , sintering , cubic zirconia , composite material , transmission electron microscopy , elastic modulus , nano , microwave , sol gel , mineralogy , analytical chemistry (journal) , ceramic , nanotechnology , chemistry , chromatography , physics , quantum mechanics
This paper reports the synthesis and characteristics of nano sized 8 mol% yttria stabilized zirconia (8YSZ). The nano sized 8YSZ powder (15 nm) has been prepared by the sol-gel technique. The phase formation was confirmed by the X-Ray Diffraction (XRD) analysis and the particle size verified by transmission electron microscope (TEM). The prepared 8YSZ green samples were sintered in a microwave furnace at 1500°C for three different holding times, such as 5, 10 and 15 min. The density of the sintered samples was measured with the Archimedes method. This method revealed 98% of theoretical density of the 8YSZ sample. The surface morphology of the sintered samples was examined by the scanning electron microscope (SEM). The mechanical properties, including nanohardness, elastic modulus and coefficient of friction of the high density sample have been evaluated.     Key words: Sol-gel, nano 8YSZ, microwave sintering, nano hardness, elastic modulus, coefficient of friction.

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