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Nanocrystalline nickel-zinc ferrites Ni 0.5 Zn 0.5 Fe 2 O 4  thin films have been synthesized via the electrodeposition-anodization from the aqueous sulfate bath. The electrodeposited (Ni-Zn)Fe 2  alloy was anodized in aqueous 1 M KOH solution to form the corresponding hydroxides which annealed at different temperatures ranging from 800 to 1000 ∘ C for various periods from 1 to 4 h, to get the required ferrite. SEM micrograph of the formed ferrite particles, annealed at 1000 ∘ C for 4 h appeared as the octahedral-like structure. A good saturation magnetization of 28.2 emu/g was achieved for Ni 0.5 Zn 0.5 Fe 2 O 4  thin film produced after the aforementioned conditions. The kinetic studies of the crystallization of Ni 0.5 Zn 0.5 Fe 2 O 4  films appeared to be first-order reaction and the activation energy was found to be 10.5 k Joule/mole.

Electrochemical Synthesis of Nanocrystalline Ni0.5Zn0.5Fe2O4 Thin Film from Aqueous Sulfate Bath

Electrochemical Synthesis of Nanocrystalline Ni_0.5Zn_0.5Fe₂O₄ Thin Film from Aqueous Sulfate Bath