Microwave-Assisted Hydrogenation of Codeine in Aqueous Media | Zendy

Fulya Taktak | Zendy; İbrahim Bulduk | Zendy

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Microwave-Assisted Hydrogenation of Codeine in Aqueous Media

Author(s) -

Fulya Taktak,

İbrahim Bulduk

Publication year - 2012

Publication title -

isrn organic chemistry

Language(s) - English

Resource type - Journals

eISSN - 2090-5157

pISSN - 2090-5149

DOI - 10.5402/2012/104975

Subject(s) - potentiometric titration , codeine , elemental analysis , chemistry , aqueous solution , aqueous medium , high performance liquid chromatography , titration , environmentally friendly , chromatography , microwave , proton nmr , nuclear chemistry , organic chemistry , computer science , medicine , ion , ecology , telecommunications , morphine , pharmacology , biology

An efficient one-pot microwave-assisted hydrogenation of codeine was achieved in aqueous solution. This technique is simple, fast, environmentally friendly, and highly efficient. Structure of produced dihydrocodeine was approved by using FT-IR, 1 H NMR, 13 C NMR, EIMS, and elemental analysis technique. Its purity analysis was performed by using HPLC and assay analysis was performed by using potentiometric titration methods.

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