Determination of Sulfonamides in Meat by Liquid Chromatography Coupled with Atmospheric Pressure Chemical Ionization Mass Spectrometry | Zendy

Dal-Ho Choi Kim | Zendy

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Determination of Sulfonamides in Meat by Liquid Chromatography Coupled with Atmospheric Pressure Chemical Ionization Mass Spectrometry

Author(s) -

Dal-Ho Choi Kim

Publication year - 2002

Publication title -

bulletin of the korean chemical society

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.237

H-Index - 59

eISSN - 1229-5949

pISSN - 0253-2964

DOI - 10.5012/bkcs.2002.23.11.1590

Subject(s) - atmospheric pressure chemical ionization , chemistry , chromatography , mass spectrometry , chemical ionization , liquid chromatography–mass spectrometry , analytical chemistry (journal) , atmospheric pressure , ionization , organic chemistry , geology , ion , oceanography

Liquid chromatography/atmospheric pressure chemical ionization-mass spectrometry (LC-APCI-MS) has been used for the determination of sulfonamides in meat. Five typical sulfonamides were selected as target compounds, and beef meat was selected as a matrix sample. As internal standards, sulfapyridine and isotope labeled sulfamethazine ( 1 3 C 6 -SMZ) were used. Compared to the results of recent reports, our result have shown improved precision to a RSD of 1.8% for the determination of sulfamethazine spiked with 75 ng/g level in meat.

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