Insights into the Electrochemistry of the Deposition of Boron from KCl-KF-NaBF4 Melt | Zendy

Rahul Pal | Zendy; S. Anthonysamy | Zendy

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Insights into the Electrochemistry of the Deposition of Boron from KCl-KF-NaBF4 Melt

Author(s) -

Rahul Pal,

S. Anthonysamy

Publication year - 2014

Publication title -

portugaliae electrochimica acta

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.252

H-Index - 27

eISSN - 1647-1571

pISSN - 0872-1904

DOI - 10.4152/pea.201406405

Subject(s) - boron , electrochemistry , deposition (geology) , materials science , chemical engineering , inorganic chemistry , chemistry , geology , organic chemistry , electrode , paleontology , sediment , engineering

Electrochemical reduction of boron from boron containing fluoroborate species present in KCl (81.54 mol%)-KF (18.45 mol%)-NaBF 4 (1.67x10 -4 mol cm -4 ) melt on a platinum electrode was studied by cyclic voltammetry and chronoamperometry. These studies were carried out over the temperature range 1073 – 1123 K. Boron-containing electroactive species is shown to reduce quasi-reversibly at low scan rates ( 0.1 V s -1 ) through a single-step three-electron

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