Electrodeposition of Iron Films and their Characterization Using Spectroscopic Techniques and Electron Microscopy | Zendy

Juan-Isidro Corredor | Zendy; Gilberto Jorge | Zendy; Cristian Rojas | Zendy

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Electrodeposition of Iron Films and their Characterization Using Spectroscopic Techniques and Electron Microscopy

Author(s) -

Juan-Isidro Corredor,

Gilberto Jorge,

Cristian Rojas

Publication year - 2009

Publication title -

portugaliae electrochimica acta

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.252

H-Index - 27

eISSN - 1647-1571

pISSN - 0872-1904

DOI - 10.4152/pea.200903329

Subject(s) - characterization (materials science) , electron microscope , materials science , electron , scanning electron microscope , microscopy , analytical chemistry (journal) , nanotechnology , chemistry , optics , composite material , physics , environmental chemistry , nuclear physics

Using chronoamperometry technique and a ferrous ammonium sulphate bath, an iron film was electroplated on a silver electrode. The characterization of the iron film was carried out using the analytical Electron Probe for Microanalysis (EPMA), X ray Diffraction (DRX) and Spectroscopy Mossbauer Transmission (TMS). The obtained results indicate that the film had an approximated thickness of 20 µm and it was compound mainly of metallic iron with crystalline structure bcc . Analysis EPMA indicated that the iron film presented islands of silver of different sizes in all the area.

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