Green synthesis of Fe$_{3}$O$_{4}$ nanoparticles by one-pot saccharide-assisted hydrothermal method | Zendy

A. Demir Korkmaz | Zendy; A. Baykal | Zendy; H. Sözeri | Zendy

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Green synthesis of Fe$_{3}$O$_{4}$ nanoparticles by one-pot saccharide-assisted hydrothermal method

Author(s) -

A. Demir Korkmaz,

A. Baykal,

H. Sözeri

Publication year - 2014

Publication title -

turkish journal of chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.239

H-Index - 46

eISSN - 1303-6130

pISSN - 1300-0527

DOI - 10.3906/kim-1401-73

Subject(s) - chemistry , maltose , lactose , nanoparticle , hydrothermal circulation , galactose , nuclear chemistry , mannose , fourier transform infrared spectroscopy , nanorod , hydrothermal synthesis , iron oxide nanoparticles , superparamagnetism , crystallite , iron oxide , inorganic chemistry , chemical engineering , crystallography , organic chemistry , sucrose , physics , magnetization , quantum mechanics , magnetic field , engineering

A saccharide-assisted hydrothermal route starting from a single iron precursor was employed to study the influence of reducing saccharides on the formation of iron oxide (Fe3O4) nanoparticles (NPs). Fe3O4 NPs, which were confirmed by X-ray diffraction analysis, were successfully synthesized by a hydrothermal method in which mannose, maltose, lactose, and galactose served as reducing agents. The formation of Fe3O4 NPs was also confirmed by Fourier transform infrared spectroscopy. Samples exhibited different crystallite sizes estimated based on line profile fitting as 12 \pm 2, 9 \pm 2, 13 \pm 3, and 9 \pm 3 nm for mannose, maltose, lactose, and galactose, respectively. Magnetic characterization results revealed superparamagnetic features of the NPs obtained with galactose, mannose, and maltose.

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