Synthesis and Characterization of Pd(II) And Pt(II) Complexes with Bis [Hg (2-Apt)] Compound. | Zendy

Beriwan Muhamad Hamad Ameen | Zendy; Hikmat Ali Mohamad | Zendy

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Synthesis and Characterization of Pd(II) And Pt(II) Complexes with Bis [Hg (2-Apt)] Compound.

Author(s) -

Beriwan Muhamad Hamad Ameen,

Hikmat Ali Mohamad

Publication year - 2018

Publication title -

kirkuk university journal-scientific studies

Language(s) - English

Resource type - Journals

eISSN - 2616-6801

pISSN - 1992-0849

DOI - 10.32894/kujss.2018.13.3.2

Subject(s) - chemistry , mole , molar conductivity , mole fraction , thiophenol , metal , inorganic chemistry , ligand (biochemistry) , salt (chemistry) , medicinal chemistry , carbon 13 nmr , nuclear chemistry , elemental analysis , stereochemistry , organic chemistry , biochemistry , receptor

The reaction of one mole of Hg(II) acetate with two mole of 2-amino thiophenol gave one mole of [Hg(2-apt)] compound. While the reaction of one mole of [Hg(2-apt)] with two moles of MCL2 salt. Produced new complexes in general formula [M2{Hg(2-apt)Cl4] where M=Pt(II) or Pd(II).All the prepared complexes were identified using FT-IR, 1H-NMR,13CNMR,elemental analyses (CHNS) and molar conductivity. The results exhibited that metal bounded to the ligand via S and N in squar planer geometries.

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