Fabrication of Nanofiltration Membrane Utilising Surfactant Via Non-Solvent Induced Phase Separation Method
Author(s) -
Rosmanisah Mohamat
Publication year - 2019
Publication title -
spektra jurnal kajian pendidikan sains
Language(s) - English
Resource type - Journals
eISSN - 2548-642X
pISSN - 2442-9910
DOI - 10.32699/spektra.v5i2.108
Subject(s) - nanofiltration , materials science , membrane , chemical engineering , exfoliation joint , solvent , raman spectroscopy , titanium dioxide , pulmonary surfactant , scanning electron microscope , graphene , layer (electronics) , filtration (mathematics) , oxide , nanotechnology , chemistry , composite material , organic chemistry , biochemistry , physics , statistics , optics , mathematics , engineering , metallurgy
In this work, graphene oxide (GO) and titanium dioxide (TiO 2 ) were used as an additive to fabricate the nanofiltration (NF) membrane. GO was synthesised via electrochemical exfoliation method utilising sodium bis(3,5,5-trimethyl-1-hexyl) sulphosuccinate (AOT4) surfactant. The synthesised GO was then used to fabricate PVDF-based NF membrane namely PVDF/GO_TiO 2 via non-solvent induced phase separation (NIPS) method. The effects of embedded GO and TiO 2 on the morphology and structural properties of PVDF/GO_TiO 2 were investigated by using field emission scanning electron microscopy (FESEM) and micro-Raman spectroscopy. The finding shows that PVDF/GO_TiO 2 present thin and dense top layer supported by macro-voids sub-layer with sponge-like layer at the bottom. Based on its morphology, the fabricated PVDF/GO_TiO 2 membrane is potential to be applied as membrane filtration for water treatment application.
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