GREEN SYNTHESIS OF COPPER OXIDE NANOPARTICLES
Author(s) -
Hanh Ngoc Nguyen,
Thao Huu Vo
Publication year - 2011
Publication title -
science and technology development journal
Language(s) - English
Resource type - Journals
ISSN - 1859-0128
DOI - 10.32508/stdj.v14i3.1965
Subject(s) - copper , calcination , nanoparticle , materials science , copper oxide , polyethylene glycol , transmission electron microscopy , scanning electron microscope , oxide , chemical engineering , metal , hydroxide , inorganic chemistry , nanotechnology , chemistry , metallurgy , organic chemistry , catalysis , composite material , engineering
Nanoparticles of metal and metallic oxides have be come a very active research area in the field of material chemistry. The surfac e effect is mainly responsible for deviation of the properties of nano-materials from that of the bulk. Nanosize copper oxide was synthesized by hydrolysi s of copper salts in basic medium using biodegradable non-ionic polymer polyethylene glycol (PEG) as surface active agent The X-ray powder diffraction p atterns (XRD) present typical peaks of copper oxides formed. The transmission electron microscopy (TEM) and scanning electron microscopy (SEM) images determined the shape and the nanosizes of th e particles of about 10-30nm. The results exhibited the role of intermediate nanosize copper hydroxide species on the formation of copper oxide nanoparticles. The influence of synthesis temperatu re, reaction time, calcination temperature, etc. wa s studied.
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