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Several per-O-acetyl and per-O-benzoyl glycosylthiocarbamides were synthesized by the interaction of glycosylisothiocyanates and o-phenylenediamine. While these thiocarbamideson further reactions with anisaldehyde give respective benzylidene derivatives. The identities of these newly synthesized compounds were established on the basis of usual chemical transformations, IR, 1 H NMR, 13 C NMR and Mass spectral studies. All the synthesized compounds have been evaluated for their antibacterial and antifungal activity against different bacteria and fungi by the agar diffusion method.

NOVEL SYNTHESIS AND CHARACTERISATION OF SOME BENZYLIDENE DERIVATIVES OF GLYCOSYL THIOCARBAMIDES