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STRUCTURAL AND THERMAL CHARACTERISTICS OF HYBRID Co(II) PEROVSKITE CRYSTALS
Author(s) -
S. Nithya,
K. Sugandhi,
P. Muthuraja,
S. Balachandar,
M. Dhandapani,
K. R. Aranganayagam
Publication year - 2018
Publication title -
rasayan journal of chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.281
H-Index - 22
eISSN - 0976-0083
pISSN - 0974-1496
DOI - 10.31788/rjc.2018.1133030
Subject(s) - perovskite (structure) , thermal , materials science , crystallography , thermodynamics , chemistry , physics
The single crystals of benzyltributylammonium tetrachloro cobaltate (II) monohydrate (BTBA-Co) crystals were grown by slow evaporation solution growth technique at room temperature. The structural characteristics of the grown crystals were studied using Fourier transform infrared (FT-IR) spectroscopy, nuclear magnetic resonance (NMR 1H and 13C) spectroscopy, powder X-ray diffraction (PXRD) and unit cell parameter analyses. Phase transitions were studied through thermal analyses (TG-DTA and DSC).

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