Synthesis & Characterization of Heterocyclic Amide Derivative via Ugi Reaction | Zendy

Osama S.Hashim | Zendy

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Synthesis & Characterization of Heterocyclic Amide Derivative via Ugi Reaction

Author(s) -

Osama S.Hashim

Publication year - 2018

Publication title -

eurasian journal of analytical chemistry

Language(s) - English

Resource type - Journals

ISSN - 1306-3057

DOI - 10.29333/ejac/99621

Subject(s) - derivative (finance) , amide , chemistry , ugi reaction , characterization (materials science) , combinatorial chemistry , stereochemistry , organic chemistry , isocyanide , materials science , nanotechnology , business , finance

Synthesis of heterocyclic amid derivative (cyclohexanecarbox-amide) by the reacting four-compound [Formaldehyde], [N-(phenethyl)formamide], [Cyclohexanecarboxylic acid], and [Creatinine] as amine source. This reaction is practical extension of (Ugi reaction). The derivatives have been performed with other catalytic agents under temp (-10°C) and the organic synthesis was monitories by TLC [thin layer chromatography] and the formation of final compound proofed by Nuclear Magnetic Resonance Spectra [1HNMR] [13CNMR] BRUKER (500MHz, CDL3), (125MHz, CDL3 and Infra-Red spectra [FTIR] (shimadzu).

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