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Yeni Ni(II) iyon-cifti kompleksi, [BzTPP][Ni(dto) 2 ] [(dto) 2 - = ditiooksalat ve (BzTPP) + = benziltrifenilfosfonyum] sentezlendi ve tek kristal X-isini kirinimi yontemi ile karakterize edildi. Kristal yapi analizi kompleksin monoklinik uzay grubu ADDIN IUCrCIF ="hk2081 _space_group_name_H-M_alt"> P2 1 /c 'de kristallendigini ve asimetrik biriminde birbirinden ayrik olarak [BzTPP] + organik katyonu ve [Ni(dto) 2 ] 2 - kompleks anyonun yarisindan olustugunu gostermektedir. Nikel atomu dort koordinatlidir ve kare duzlem koordinasyon geometrisine sahiptir. Kristal yapida, organik katyonlar ve inorganik anyonlar molekuller arasi C–H···O hidrojen baglariyla ve C–H···π ve π−π etkilesimleriyle birbirlerine baglanirlar, buda uc boyutlu kristal yapinin olusmasini ve kafes yapinin kararliligini saglar.

Synthesis and 3D crystal structure of new Ni(II)-ion-pair complex