Preparation and Characterization of TiO2 Nanostructure by TiCl4 Hydrolysis with Additive NaOH | Zendy

Rashed Taleb Rasheed | Zendy

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Preparation and Characterization of TiO2 Nanostructure by TiCl4 Hydrolysis with Additive NaOH

Author(s) -

Rashed Taleb Rasheed

Publication year - 2018

Publication title -

al-mustansiriyah journal of science

Language(s) - English

Resource type - Journals

eISSN - 2521-3520

pISSN - 1814-635X

DOI - 10.23851/mjs.v28i2.506

Subject(s) - sodium hydroxide , scanning electron microscope , nanostructure , titanium dioxide , hydrolysis , materials science , chemical engineering , infrared spectroscopy , nanoparticle , spectroscopy , hydroxide , morphology (biology) , nuclear chemistry , nanotechnology , chemistry , inorganic chemistry , organic chemistry , composite material , physics , quantum mechanics , biology , engineering , genetics

Titanium dioxide (TiO2) nanostructures were synthesized via the hydrolysis of TiCl4 in alcohol / water solution/with sodium hydroxide solution in the ice-bath (0-5 ◦C). The particles were char-acterized by using X-ray diffraction technique (XRD), spectroscopy of Ultra Violet-Visible (UV / Visible) and infrared (FT-IR), atomic force microscope (AFM) and scanning electron micro-scope (SEM) analysis were used in order to gain information about the material, morphology, size and the shape of the particles

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