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Thermal decomposition of Co(II) complex with N-benzyloxycarbonylglycinato   ligand, [Co(N-Boc-gly)2(H2O)4]•2H2O, in non-isothermal conditions occurs in   three complex steps. In order to investigate detail kinetics of first two   steps, dehydration and ligand degradation, DTG curves were deconvoluted using   product of Gaussian and Lorentzian function. It was shown that process of   complex dehydration consists of three, while process of ligand fragmentation   consist of five elementary steps. For elementary steps the kinetic triplet   (Ea, Z and f(α)) was determinated. Kinetic parameters were obtained by   application of IKP method. On the basis of Màlek’s criteria and   Šesták-Berggren's method, Šesták-Berggren's model, f(α)=αM(1-α)N was   suggested for all elementary steps, while Master plot method and Perez-   Maqueda criteria confirmed suggested reaction models. The thermodynamic   activation parameters were calculated for process of complex dehydration, and   lifetime for first elementary step of the dehydration and ligand degradation   processes was estimated. [Projekat Ministarstva nauke Republike Srbije, br. 172055

Kinetics of multi-step processes of thermal degradation of Co(II) complex with N-benzyloxycarbonylglycinato ligand. Deconvolution of DTG curves