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High pressure sintered ZrO2-6%wt REO
Author(s) -
Carlos Kuranaga,
Guerold S. Bobrovnitchii
Publication year - 2007
Publication title -
science of sintering
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.309
H-Index - 25
eISSN - 1820-7413
pISSN - 0350-820X
DOI - 10.2298/sos0701017k
Subject(s) - sintering , materials science , tetragonal crystal system , fracture toughness , phase (matter) , oxide , high pressure , volume (thermodynamics) , toughness , metallurgy , composite material , mineralogy , chemistry , thermodynamics , organic chemistry , physics
The sintering conditions employed in this work are innovative, due to the use of an alternative technology to process ZrO2-REO (rare earth oxide mixture), so called high temperature - high pressure (HPHT). A pressure of 5GPa was used, temperatures of 1100, 1200, and 1300 o C, for times of 2 and 5 minutes. The best results were obtained for samples sintered at 5GPa/1300 o C/5min., where a micro-hardness of 4.8GPa, fracture toughness of 5.3MPa.m ½, density of 97.9%, and 88% in volume of a tetragonal phase retained at room temperature were achieved

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