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Synthesis and characterization of mesoporous α-Fe2O3 nanoparticles and investigation of electrical properties of fabricated thick films
Author(s) -
Ali Mirzaei,
K. Janghorban,
B. Hashemi,
Seyyed Abbas Hosseini,
Maryam Bonyani,
Salvatore Gianluca Leonardi,
A. Bonavita,
G. Neri
Publication year - 2016
Publication title -
processing and application of ceramics
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.326
H-Index - 15
eISSN - 2406-1034
pISSN - 1820-6131
DOI - 10.2298/pac1604209m
Subject(s) - materials science , calcination , mesoporous material , ethylene glycol , nanoparticle , chemical engineering , citric acid , polymerization , nanotechnology , polymer , composite material , catalysis , organic chemistry , chemistry , engineering
In this work, α-Fe2O3 nanoparticles (NPs) have been synthesized by using a simple Pechini sol-gel method from iron nitrate, citric acid as complexing agent and ethylene glycol as polymerization agent. The calcined α-Fe2O3 NPs were fully characterized by different techniques. It was confirmed that ultrafine and highly crystalline α-Fe2O3 NPs with high purity and mesoporous nature can be obtained after calcination at 550 °C for 3 h. In addition, the results of electrical resistance measurements of the fabricated Fe2O3 thick films showed that α-Fe2O3\udthick films have stable electrical properties which are beneficial for electrical applications such as gas sensing and field effect transistors

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