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Silicon electrodeposition on glassy carbon from the KF-KCl-K2SiF6, KF-KCl-K2SiF6-KOH and KF-KCl-K2SiF6-SiO2 melts was studied by the cyclic   voltammetry. Тhe electroreduction of Si(IV) to metallic Si was observed as a   single 4-electron wave under all considered conditions. The reactions of   cathode reduction of silicon from fluoride and oxyfluoride complexes were   suggested. It was shown that the process can be controlled by the preliminary   transformation of SiO44- to SiF62- and SiOxFyz-. The influence of the current   density on structure and morphology of silicon deposits obtained during   galvanostatic electrolysis of the KF-KCl-K2SiF6-SiO2 melt was studied

Silicon electrodeposition from chloride-fluoride melts containing K2SiF6 and SiO2