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A multi-step thermal decomposition of a molecular precursor,  {N(n-C4H9)4[FeIIFeIII(C2O4)3}∞ has been studied using non-isothermal  thermogravimetry (TG) measurements in the temperature range 300 to ~800 K at  multiple heating rates (5, 10 and 20 K min-1). The thermal decomposition of  the oxalate-based complex proceeds stepwise through a series of intermediate  reactions. Two different isoconversional methods, namely, improved iterative  method and model-free method are employed to evaluate the kinetic parameters:  activation energy and rate of reaction, and the most probable reaction  mechanism of thermal decomposition is also determined. The different reaction  pathways leading to different steps in the TG profile have also been explored  which are supplemented by earlier experimental observations of the present  authors

Thermal decomposition of a molecular material {N(n-C4H9)4[FeIIFeIII(C2O4)3]}∞ leading to ferrite: A reaction kinetics study