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A new type of complexes compounds (NH 4 ) 6 [M 3 Fe 5 (C 4 O 5 H 4 ) 6 (C 4 O 5 H 3 ) 6 ] 16H 2 O (where M(III) = Y, Eu, Gd, Er), (NH 4 ) 6 [M 3 Fe 5 (C 4 O 6 H 4 ) 6 (C 4 O 6 H 3 ) 6 ]. 16H 2 O (where M(III) = Gd, Er) and (NH 4 ) 6[M 3 Fe 5 (C 6 O 7 H 1 0 ) 6 (C 6 O 7 H 9 ) 6 ] xH 2 O (where M(III) = Y; x = 8; M(III) = Eu, Er; x = 22) [C 4 O 5 H 4 2 = malate anion; C 4 O 4 H 4 2 - = tartaratc anion, C 6 O 7 H 1 1 = gluconate anion] have been synthesized and characterised by elemental chemical analysis and physico-chemical measurements (1R, UV-Vis spectroscopy and magnetic determinations). The synthetic possibilities offered by the use of these new compounds as potential precursors for garnets have been suggested.

Polynuclear coordination precursors compounds for M3Fe5O12 garnets (M=Y, Eu, Gd and Er), Part I: Synthesis of the precursors