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The synthesis, characterization and a thermal (TG and DSC) study of the coordination compounds Gd(MS) 3 (py-NO) 2 , Gd(MS) 3 .(2-picNO) 2 , Gd(MS)3 (3-picNO) 2 , Gd(MS)3 (4-picNO) 2 , Lu(MS) 3 .(py-NO) 2 .2H 2 O, Lu(MS) 3 .(2-picNO) 1 . 5 .H 2 O, Lu(MS) 3 (3-picNO) and Lu(MS) 3 .(4-picNO) 2 are reported (MS = methanesulfonate, py-NO = pyridine-N-oxide, 2-picNO, 3-picNo and 4-picNO are 2-, 3- and 4-picoline-N-oxides, respectively). The observed thermal stability trend is: 2-picNO < py-NO < 4-picNO < 3-picNO for Gd and 2-picNO < 4-picNO < 3-picNO < py-NO for Lu. It was shown that the release of ligand molecules (endothermic) is followed by the thermal degradation of the ligands (exothermic).

journal of the serbian chemical society

Synthesis, characterization and a thermal (TG-DSC) study of gadolinium and lutetium methanesulfonate coordination compounds with pyridine-N-oxide and 2-, 3- and 4-picoline-N-oxides