Ca(II) complexes of tetraazamacrocycles derived from 3, 4-hexenedione and diaminoalkanes | Zendy

R. N. Prasad | Zendy; M. Agrawal | Zendy; Sangeeta Malhotra | Zendy

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Ca(II) complexes of tetraazamacrocycles derived from 3, 4-hexenedione and diaminoalkanes

Author(s) -

R. N. Prasad,

M. Agrawal,

Sangeeta Malhotra

Publication year - 2004

Publication title -

journal of the serbian chemical society

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.227

H-Index - 45

eISSN - 1820-7421

pISSN - 0352-5139

DOI - 10.2298/jsc0409661p

Subject(s) - chemistry , elemental analysis , spectroscopy , conductance , polymer chemistry , nuclear magnetic resonance spectroscopy , medicinal chemistry , stereochemistry , inorganic chemistry , physics , quantum mechanics , condensed matter physics

Ca(II) macrocyclic complexes [(Et 4 [n]tetraeneN 4 )CaX 2 ] (where n = 14. 16, 20. 24, 32, X = Cl - , NCS - ) have been synthesized via cyclocondensation of 3,4-hexanedione with aliphatic diamines, such as 1,3-diaminopropane, 1,4-diaminobutane. 1,6-diaminohexane, 1,8-diaminooctane or 1,12-diaminododecane. The synthesized complexes were characterized by elemental analyses, conductance measurements and IR and 1 H-NMR spectroscopy.

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