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Template condensation of α-diketones. such as 3,4-hexanedione or benzil, with 1,n-diaminoalkanes (where n=4, 5, 6, 7, 8, 9, 10 or 12) in the presence of Mn(II) resulted in the formation of complexes of the type [MnL(NO 3 )]NO 3 (where L = 16 to 32-membered macrocycle). These complexes have been characterized by elemental analyses, conductances, magnetic measurements, as well as IR and electronic spectra.

Termplate synthesis of Mn(II) complexes of tetraazamacrocycles derived from diaminoalkanes and 3, 4-hexanedione or benzil