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Silver nanoparticles (Ag-NPs) were prepared by wet synthesis. The Ag-NPs  suspension and the copper substrate plate were used for a preparation of  substrate-nanoparticle-substrate samples. The sandwich like samples Cu/Ag/Cu  were prepared and investigated in-situ at the isothermal external conditions  (IEC) and inside apparatus for simultaneous thermal analysis STA409 (DSC).  The in-situ results of the electrical resistance were recorded during the  Cu/Ag/Cu (IEC) sample preparation and heat treatment. Thermal effects of the  Ag-NPs sintering between copper substrates were measured by differential  scanning calorimetry (DSC) under different atmospheres. The prepared Cu/Ag/Cu  sandwich samples were characterised by means of both optical and electron  microscopy. The process of the low temperature sintering inside calorimeter  of the Ag-NPs was monitored using both thermogravimetry (TG) and DSC  technique under inert gas and under synthetic air. The exothermic heat effect  of nanosilver sintering was evaluated

Silver nanoparticles sintering at low temperature on a copper substrate: In situ characterization under inert atmosphere and air