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In this study CuO nanoparticles were prepared via direct thermal  decomposition method using basic copper sulphates as wet chemically  synthesized precursor which was calcined in air at 750°C for 2h. Samples  were characterized by thermogravimetric (TG-DSC), X-ray diffraction (XRD),  energy dispersive spectroscopy (EDS), infrared spectrum (IR), scanning  electron microscopy (SEM), and transmission electron microscopy (TEM). The  XRD, EDS, and IR results indicated that the synthesized CuO particles were  pure. The SEM and TEM results showed that the CuO nanoparticles were of  approximate spherical shape, and 170±5 nm in size. Using this method, Cuo  nanoparticles could be produced without using organic solvent, expensive raw  materials, and complicated equipment

A novel technique to synthesis of tenorite (CuO) nanoparticles from low concentration CuSO4 solution