Synthesis and Characterization a New 1,3-Diazepine Compounds from New Bis 4-Amino-3-Mercpto-1,2,4-Triazole Derivatives | Zendy

Atyaf AQ. Younus | Zendy; Nasreen R. Jber | Zendy

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Synthesis and Characterization a New 1,3-Diazepine Compounds from New Bis 4-Amino-3-Mercpto-1,2,4-Triazole Derivatives

Author(s) -

Atyaf AQ. Younus,

Nasreen R. Jber

Publication year - 2017

Publication title -

journal of al-nahrain university-science

Language(s) - English

Resource type - Journals

eISSN - 2519-0881

pISSN - 1814-5922

DOI - 10.22401/jnus.20.2.01

Subject(s) - hydrazine (antidepressant) , hydrazide , isatin , chemistry , hydrate , 1,2,4 triazole , elemental analysis , ethanol , proton nmr , triazole , fourier transform infrared spectroscopy , medicinal chemistry , organic chemistry , nuclear chemistry , polymer chemistry , physics , chromatography , quantum mechanics

Compounds with two triazole rings IVa,b were synthesized through the reaction of diacid hydrazide firstly with CS2/KOH, and secondly with excess of hydrazine hydrate. The one-step reaction of isatin with benzylidene benzeneamine (S1–S10) in ethanol gave 2-Ar-3Ar'[3,4b][1,3]benzodiazepine-4,5-diones (D1-D10) in good yields. The products were characterized using FTIR, 1 HNMR spectroscopy and CHN elemental analyses. [DOI: 10.22401/JUNS.20.2.01]

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