SYNTHESIS OF SECONDARY ALCOHOL COMPOUNDS FROM SAFROLE AND METHYLEUGENOL | Zendy

Hanoch Julianus Sohilait | Zendy; Hardjono Sastrohamidjojo | Zendy; Sabirin Matsjeh | Zendy

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SYNTHESIS OF SECONDARY ALCOHOL COMPOUNDS FROM SAFROLE AND METHYLEUGENOL

Author(s) -

Hanoch Julianus Sohilait,

Hardjono Sastrohamidjojo,

Sabirin Matsjeh

Publication year - 2010

Publication title -

indonesian journal of chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.273

H-Index - 14

eISSN - 2460-1578

pISSN - 1411-9420

DOI - 10.22146/ijc.21885

Subject(s) - chemistry , safrole , alcohol , sodium borohydride , organic chemistry , primary alcohol , cinnamyl alcohol , isopropyl alcohol , proton nmr , isoeugenol , cinnamaldehyde , eugenol , methanol , chromatography , catalysis

Synthesis of secondary alcohols compound from safrole and methyleugenol has been achieved through conVersion of allyl group to alcohol.The reaction of safrole and methyleugenol with mercuric acetate in aqueous tetrahydrofuran, followed by in situ reduction of the mercurial intermediate by alkaline sodium borohydride produced secondary alcohol namely safryl alcohol (71.25%) and methyleugenil alcohol (65.56%). The structure elucidation of these products were analyzed by FTIR, H-NMR, C-NMR and MS.

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