DEVELOPING METHOD OF DIFFERENTIAL PULSE POLAROGRAPHIC FOR ANALYSIS OF CHLORAMPHENICOL RESIDUE IN MILK | Zendy

Daryono Hadi Tjahjono | Zendy; Amir Musadad | Zendy; Septy Mariana K | Zendy

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DEVELOPING METHOD OF DIFFERENTIAL PULSE POLAROGRAPHIC FOR ANALYSIS OF CHLORAMPHENICOL RESIDUE IN MILK

Author(s) -

Daryono Hadi Tjahjono,

Amir Musadad,

Septy Mariana K

Publication year - 2010

Publication title -

indonesian journal of chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.273

H-Index - 14

eISSN - 2460-1578

pISSN - 1411-9420

DOI - 10.22146/ijc.21872

Subject(s) - polarography , chemistry , dropping mercury electrode , residue (chemistry) , electrode , detection limit , chloramphenicol , electrolyte , chromatography , pulse (music) , analytical chemistry (journal) , inorganic chemistry , voltage , biochemistry , electrochemistry , antibiotics , physics , quantum mechanics

A differential pulse polarographic method for a quantitative analysis of chloramphenicol residue in milk had been developed. Result showed that the method using dropping mercury electrode as working electrode, Ag/AgCl electrode as reference electrode, and platinum electrode as auxiliary electrode with an acetic buffer solution of pH 4.7 as supporting electrolyte had a recovery for chloramphenicol of (96.88 ± 3.17)% with a detection limit of 0,027 μg/mL, a quantitation limit of 0,089 μg/mL, and a determination limit of

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