THE SULFONATION STUDY OF REACTION MECHANISM ON PAPAVERINE ALKALOID BY GC-MS AND FT-IR | Zendy

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THE SULFONATION STUDY OF REACTION MECHANISM ON PAPAVERINE ALKALOID BY GC-MS AND FT-IR

Author(s) -

I Made Sudarma

Publication year - 2010

Publication title -

indonesian journal of chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.273

H-Index - 14

eISSN - 2460-1578

pISSN - 1411-9420

DOI - 10.22146/ijc.21715

Subject(s) - chemistry , papaverine , alkaloid , stereochemistry , chromatography , medicine

The aim of this research was to prove theoretical mechanism reaction on the sulfonation of papaverine alkaloid and the result could be used as a reference on the transformation of these alkaloid to the other derivatives. Theoriticaly sulfonation of papaverine (1) by HO-SO2Cl could produced papaverine sulfonyl chloride (1a). The formation of this product was analyzed by analytical thin layer chromatography GC-MS, and FT-IR. These analysis showed the formation of product (1a) more favorable than the other. Tlc showed product (1a) less polar than papaverine, and supported by GC-MS and infrared which showed molecular ion at m/z 412 due to the presence of – SO2Cl and vibration at 1153,4 dan 1265,2 Cm due to absorption of sulfonyl group.

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