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Fundamental studies of reactive intermediates in homogeneous catalysis. Final technical report

Publication year - 1998

Publication title -

osti oai (u.s. department of energy office of scientific and technical information)

Language(s) - English

Resource type - Reports

DOI - 10.2172/656627

Subject(s) - triple quadrupole mass spectrometer , common emitter , chemistry , ionization , mass spectrometry , volumetric flow rate , tandem , selected reaction monitoring , chromatography , quadrupole mass analyzer , ion , homogeneous , analytical chemistry (journal) , electrospray ionization , tandem mass spectrometry , nanotechnology , materials science , optoelectronics , organic chemistry , physics , quantum mechanics , thermodynamics , composite material

The chief aims during the contract period were to design, construct and implement a new flowing afterglow-guided ion beam instrument for use in determining thermochemical properties of organometallic species pertinent to homogeneous catalysis, and to develop an electrospray ionization (ESI) source for the flowing afterglow-triple quadrupole apparatus for use in real-time analysis of reactive intermediates in catalytically active solutions. Both goals were achieved. In parallel with development of the guided ion beam and electrospray ionization experiments, the author used existing equipment to work on some of the problems outlined in the previous proposal, and to open up new research areas. A summary of research activities and publications acknowledging DOE support follows

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