Synthesis of model compounds for coal liquefaction research: Final report, June 21, 1990--July 30, 1993 | Zendy

A.S. Hirschon | Zendy; Marianna Asaro | Zendy; Jeffrey C. Bottaro | Zendy

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Synthesis of model compounds for coal liquefaction research: Final report, June 21, 1990--July 30, 1993

Author(s) -

A.S. Hirschon,

Marianna Asaro,

Jeffrey C. Bottaro

Publication year - 1993

Publication title -

osti oai (u.s. department of energy office of scientific and technical information)

Language(s) - English

Resource type - Reports

DOI - 10.2172/61099

Subject(s) - prime (order theory) , dibenzothiophene , prime time , coal liquefaction , coal , computer science , chemistry , sulfur , organic chemistry , mathematics , combinatorics , telecommunications

The objectives of this project were to develop feasible synthetic routes to produce (1) 4(4{prime}-hydroxy-5{prime}6{prime},7{prime}8{prime}-tetrahydro-1{prime}-naphthylmethyl)-6-methyldibenzothiophene, and (2) a 1-hydroxynaphthalene-dibenzothiophene polymer. These compounds are thought to be representative of sulfur containing molecules in coal. The program was divided into two technical tasks. Unfortunately, the attempted syntheses of these compounds was unsuccessful due to their unusual reactivities. Attempted synthetic routes and possible future routes are described, and Appendix A lists the compounds that were synthesized during this program

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