z-logo
open-access-imgOpen Access
Evaluation of microwave digestion systems for mercury recovery in an oil matrix
Author(s) -
M.J. Whitaker,
J.W. Clymire
Publication year - 1997
Publication title -
osti oai (u.s. department of energy office of scientific and technical information)
Language(s) - English
Resource type - Reports
DOI - 10.2172/569056
Subject(s) - mercury (programming language) , microwave , microwave digestion , process engineering , matrix (chemical analysis) , dissolution , computer science , materials science , chemistry , environmental science , engineering , chromatography , detection limit , chemical engineering , telecommunications , programming language
The scope of this document is to characterize three microwave systems developed by CEM Corporation. The purpose of this investigative work was to evaluate the performance of each system for dissolution qualities and the recovery of mercury in an oil based matrix. The microwave systems evaluated were the heavy duty vessel system (HDV), the advanced composite system (ACV), and the open vessel system (OVS). All three systems have automated features, but all systems are limited by one factor or another. EPA method 3051 was the procedure used for sample preparation for this project. This particular microwave digestion method can also be used for other metal analytes of interest. Of the three different systems, only the HDV (now UDV) demonstrated complete digestion of the oil based matrix in a one step process and acceptable mercury recoveries

The content you want is available to Zendy users.

Already have an account? Click here to sign in.
Having issues? You can contact us here
Accelerating Research

Address

John Eccles House
Robert Robinson Avenue,
Oxford Science Park, Oxford
OX4 4GP, United Kingdom