Open AccessSynthesis of picryl chloride
Author(s) -
D.V. Hayes,
F.I. Honea
Publication year - 1970
Publication title -
osti oai (u.s. department of energy office of scientific and technical information)
Language(s) - English
Resource type - Reports
DOI - 10.2172/532469
Subject(s) - picryl chloride , yield (engineering) , chemistry , chloride , chromatography , toxicology , organic chemistry , materials science , metallurgy , medicine , biology , immune system , immunology
A total of six pilot-scale batches of picryl chloride were made. These included three 5-kg batches and three 10-kg batches. The three 5-kg batches were made to investigate the problems encountered with actual production and materials handling. The three 10-kg batches were made to study the process parameters and the yield problems originally encountered with the 5-kg batches. The yields on the 5-kg batches ranged from 40 to 60% of approximately 50% purity. The yields on the 10-kg batches were 80, 86 and 91% in chronological order. The purities were 95, 99+ and 99+% respectively
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