Analysis of Rare Earth Elements in Geologic Samples using Inductively Coupled Plasma Mass Spectrometry; US DOE Topical Report - DOE/NETL-2016/1794 | Zendy

Tracy L. Bank | Zendy; Elliot Roth | Zendy; Phillip Tinker | Zendy; Evan Granite | Zendy

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Analysis of Rare Earth Elements in Geologic Samples using Inductively Coupled Plasma Mass Spectrometry; US DOE Topical Report - DOE/NETL-2016/1794

Author(s) -

Tracy L. Bank,

Elliot Roth,

Phillip Tinker,

Evan Granite

Publication year - 2016

Publication title -

osti oai (u.s. department of energy office of scientific and technical information)

Language(s) - English

Resource type - Reports

DOI - 10.2172/1415779

Subject(s) - inductively coupled plasma mass spectrometry , mass spectrometry , certified reference materials , oil shale , rare earth element , rare earth , inductively coupled plasma , chemistry , sample preparation , analytical chemistry (journal) , chromatography , mineralogy , engineering , plasma , waste management , detection limit , physics , quantum mechanics

Inductively Coupled Plasma Mass Spectrometry (ICP-MS) is used to measure the concentrations of rare earth elements (REE) in certified standard reference materials including shale and coal. The instrument used in this study is a Perkin Elmer Nexion 300D ICP-MS. The goal of the study is to identify sample preparation and operating conditions that optimized recovery of each element of concern. Additionally, the precision and accuracy of the technique are summarized and the drawbacks and limitations of the method are outlined.

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