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Synthesis and application of magnetized nanoparticles to remove lead from drinking water: Taguchi design of experiment
Author(s) -
Muhammad Irfan Jalees
Publication year - 2020
Publication title -
journal of water sanitation and hygiene for development
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.414
H-Index - 22
eISSN - 2408-9362
pISSN - 2043-9083
DOI - 10.2166/washdev.2020.097
Subject(s) - taguchi methods , fourier transform infrared spectroscopy , sorption , adsorption , exothermic reaction , chemistry , nanoparticle , nuclear chemistry , chemical engineering , materials science , analytical chemistry (journal) , environmental chemistry , nanotechnology , engineering , organic chemistry , composite material
Contamination in drinking water from heavy metals like Pb2+ has severe effects on health. In this study, potato peel (PP) was used as the substrate and magnetic iron nanoparticles (MI) were deposited on PP using a co-precipitated method. Fourier transformation infrared spectroscopy (FTIR) and X-ray diffraction (XRD) analysis confirmed the deposition of MI on PP. The L16 (4^4) method of Taguchi design of experiment (DOE) was used for the optimization of adsorption condition, i.e., at 6 pH, 10 min of contact time, and a dose of 15 g/L can give more than 90% removal efficiency of Pb2+ using PP-MI. Contour maps, Taguchi response analysis, and analysis of variance (ANOVA) suggested that pH has a dominant contribution in the removal of Pb2+. The adsorption process was favorable, spontaneous, and exothermic in nature and was followed by pseudo second order kinetics. A comparison of the sorption capacity of PP-MI for Pb2+ with literature values suggested that PP-MI has good potential for the removal of Pb2+. This article has been made Open Access thanks to the generous support of a global network of libraries as part of the Knowledge Unlatched Select initiative.

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