Synthesis and Characterization of Multishapes of Fe3O4 Nanoparticle by Solve-Hydrothermal Method Using Microwave Radiation | Zendy

Ahlam Jameel Abdulghani | Zendy; Waleed Madhloom Al-Ogedy | Zendy

Open Access

Synthesis and Characterization of Multishapes of Fe3O4 Nanoparticle by Solve-Hydrothermal Method Using Microwave Radiation

Author(s) -

Ahlam Jameel Abdulghani,

Waleed Madhloom Al-Ogedy

Publication year - 2016

Publication title -

baghdad science journal

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.167

H-Index - 6

eISSN - 2411-7986

pISSN - 2078-8665

DOI - 10.21123/bsj.2016.13.2.0331

Subject(s) - hydrothermal circulation , nanoparticle , scanning electron microscope , ammonium bromide , materials science , nuclear chemistry , microwave , chemical engineering , hydrothermal synthesis , metal , fourier transform infrared spectroscopy , ferrous , oleic acid , powder diffraction , nanotechnology , chemistry , crystallography , metallurgy , composite material , pulmonary surfactant , biochemistry , physics , quantum mechanics , engineering

Iron oxide(Fe3O4) nanoparticles of different sizes and shapes were synthesized by solve-hydrothermal reaction assisted by microwave irradiation using ferrous ammonium sulfate as a metal precursor, oleic acid as dispersing agent, ethanol as reducing agent and NaOH as precipitating agent at pH=12. The synthesized Fe3O4 nano particles were characterized by X-ray diffraction (XRD), FTIR and thermal analysis TG-DTG. Sizes and shapes of Fe3O4 nanoparticles were characterized by Scanning Electron Microscopy (SEM), and atomic force microscopy (AFM).

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