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A series of palladium(II) complexes from monodentate phosphine ligands ( 1a-4a ) were successfully prepared and characterized with 1 H, 31 P, 13 C NMR, and HRMS techniques. These pre-catalysts were applied for the Suzuki -Miyaura C-C coupling reaction of phenylboronic acid with bromobenzene and the influence of the base and solvent on the performance of the pre-catalysts was investigated. Sterically hindered and electronically deactivated aryl bromides as well as activated ones gave the corresponding coupling products in good to excellent yields at room temperature.

Palladium(II) Complexes of Monodentate Phosphine Ligands and Their Application as Catalyst in Suzuki-Miyaura C-C Coupling Reaction at Room Temperature