RADICAL COPOLYMERIZATION OF ACRLOYLMORPHOLINE WITH 2-HYDROXYETHYL METHACRYLATE: MONOMER REACTIVITY RATIOS AND THERMAL PROPERTIES | Zendy

Mehmet Mürşi̇t Temüz | Zendy

Open Access

RADICAL COPOLYMERIZATION OF ACRLOYLMORPHOLINE WITH 2-HYDROXYETHYL METHACRYLATE: MONOMER REACTIVITY RATIOS AND THERMAL PROPERTIES

Author(s) -

Mehmet Mürşi̇t Temüz

Publication year - 2017

Publication title -

anadolu university journal of science and technology-a applied sciences and engineering

Language(s) - Turkish

Resource type - Journals

ISSN - 1302-3160

DOI - 10.18038/aubtda.306626

Subject(s) - copolymer , azobisisobutyronitrile , monomer , polymer chemistry , thermogravimetric analysis , methacrylate , reactivity (psychology) , radical polymerization , tetrahydrofuran , materials science , polymerization , radical initiator , chemistry , organic chemistry , polymer , medicine , alternative medicine , pathology , solvent

Poli (akriloilmorfolin-co-2-hidroksietil metakrilat) geleneksel serbest radikal polimerizasyonu ile hazirlandi. Akriloilmorfolin (ACM) ve 2-hidroksietil metakrilat (HEMA) monomerleriyle kopolimerizasyon, baslatici olarak 2,2'-azobisizobutironitril (AIBN) kullanilarak 60 ° C'de tetrahidrofuran cozeltisi icinde gerceklestirildi. Kopolimerler, FT-IR, 1H ve 13C nukleer manyetik rezonans (NMR) ile karakterize edildi. Kopolimerlerin monomer bilesimleri, elemental analizin azot sonuclariyla tahmin edildi. Kopolimerdeki ACM(r 1 ) ve HEMA(r 2 ) monomerlerinin reaktivite oranlari, cesitli yontemlerle hesaplandi . Bu yontemlere gore, r 1 degeri 1.73-2.01 ve r 2 degeri 0.48-0.74'tur. Kopolimerlerin termal ozelliklerini arastirmak icin Termogravimetrik analiz kullanildi.

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