Determination of Polycyclic Aromatic Hydrocarbons Level in Commercial Turkish Milks | Zendy

Sibel Kaçmaz | Zendy

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Determination of Polycyclic Aromatic Hydrocarbons Level in Commercial Turkish Milks

Author(s) -

Sibel Kaçmaz

Publication year - 2018

Publication title -

cumhuriyet science journal

Language(s) - Turkish

Resource type - Journals

eISSN - 2587-246X

pISSN - 2587-2680

DOI - 10.17776/csj.443430

Subject(s) - repeatability , detection limit , pasteurization , chemistry , european union , chromatography , raw milk , environmental chemistry , food science , business , economic policy

Bu calismada, ticari olarak satilan Turk sutlerinde polisiklik aromatik hidrokarbon (PAH) varligi arastirilmistir. Cig sut (n = 2), pastorize sut (n = 5), UHT sut (n = 17) ve ayrica bitki sutu (n = 3) olmak uzere toplam 27 ticari sut orneginde, 4 AB oncelikli polisiklik aromatik hidrokarbon (PAH) yuksek performans sivi kromatografisi-floresans dedektor kullanilarak (HPLC-FLD) tayin edilmistir. Yontem, dogrusallik, kesinlik (tekrarlanabilirlik ve orta kesinlik), Tespit Limiti (LOD) ve Tayin Limiti (LOQ), geri kazanim ve ayrica olcum belirsizligi gibi validasyon parametreleri kullanilarak dogrulanmistir. Dort AB oncelikli PAH (4PAH) toplaminin ortalama konsantrasyonlari, cig, pastorize, UHT ve bitki sutleri icin, sirasiyla 0.10 ±0.06, 0.71 ±0.33, 0.84 ±0.57 ve 0.20 ±0.28 µg kg -1 olarak bulunmustur. Analiz edilen sut ornekleri, Benzopiren (BaP) ve 4 AB oncelikli poliaromatik hidrokarbon (4PAH) icin Avrupa Birligi tarafindan belirlenen 1.0 µg kg -1 'lik maksimum limitlerin altinda oldugu gorulmustur.

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