Two-dimensional J-resolved nuclear magnetic resonance spectral study of two bromobenzene glutathione conjugates. | Zendy

James A. Ferretti | Zendy; R. J. Highet | Zendy; L R Pohl | Zendy; Terrence J. Monks | Zendy; J. A. Hinson | Zendy

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Two-dimensional J-resolved nuclear magnetic resonance spectral study of two bromobenzene glutathione conjugates.

Author(s) -

James A. Ferretti,

R. J. Highet,

L R Pohl,

Terrence J. Monks,

J. A. Hinson

Publication year - 1985

Publication title -

environmental health perspectives

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 2.257

H-Index - 282

eISSN - 1552-9924

pISSN - 0091-6765

DOI - 10.1289/ehp.8561139

Subject(s) - bromobenzene , coupling constant , nuclear magnetic resonance , nuclear magnetic resonance spectroscopy , proton , chemistry , molecule , glutathione , physics , nuclear physics , biochemistry , organic chemistry , particle physics , catalysis , enzyme

The application of two-dimensional J-resolved nuclear magnetic resonance spectroscopy to determine the structure of two bile metabolites isolated from rats injected interperitoneally with bromobenzene is described. The structures of the two molecules are obtained unambiguously from the proton-proton spin coupling constants. This paper discusses the fundamentals of the technique and demonstrates the resolution of small long-range coupling constants.

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