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Synthesis of Copper Sulfide Nanowhisker via Sonochemical Way and its Characterization
Author(s) -
Changqi Xu,
Zhicheng Zhang,
Qiang Ye,
Xiong Liu
Publication year - 2003
Publication title -
chemistry letters
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.492
H-Index - 114
eISSN - 1348-0715
pISSN - 0366-7022
DOI - 10.1246/cl.2003.198
Subject(s) - chemistry , copper , characterization (materials science) , sulfide , copper sulfide , nanotechnology , organic chemistry , materials science
An ultrasonic irradiation route (USI route) is developed to synthesize whisker-like copper sulfide (Cu9S8) nanocrystals via the reaction between copper sulfate pantahydrate (CuSO4·5H2O) and thioacetamide (CH3CSNH2) in an aqueous solution at room temperature under ambient pressure. XRD, TEM, UV–vis and PL spectra are used to characterize the obtained product. A possible reaction process is suggested in the end of this paper.

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